Facilities

The Poerschke research group has approximatley 1250 sq. ft. of dedicated research space split between labs in Amundson 206 and 250. We are currently developing facilitites to perform a variety of materials synthesis, processing, and environmental testing protocols. We also have easy access to various analytical instruments (XRD, SEM, TEM, etc) in the UMN CharFac

Major Equipment

Equipment

Visual Reference

Specifications & Capabilities

Vacuum Annealing Furnace and Hot Press
Oxy-gon vacuum furnace mounted on a Carver hydraulic press, showing front view, internal chamber, and control panel
  • Oxy-gon vacuum furnace installed on a Carver hydraulic press. 
  • Tungsten mesh elements and heat shields enable operating up to 2000 oC in vacuum or inert atmosphere. 
  • Turbomolecular pump used to rapidly achieve high vacuum conditions in chamber.
  • Can be operated as an annealing furnace (no pressure) or as a hot press with open compression platens or a closed die.  
Vacuum Arc Melter
Arcast Arc 200 cold crucible arc melter showing main unit, power supply setup, and close-up of copper crucible.
  • Arcast Arc 200 cold crucible arc melting and casting furnace. 
  • Tungsten electrode powered by 600 A DC power supply used to general arc to melt a variety of metal alloys. 
  • Main crucible has capacity to melt 200 g of material and is equipped with electromagnetic stirring system to improve alloy homogenization. 
  • System is equipped with tilt casting, suction casting, centrifugal casting, and button casting crucibles to enable a variety of sample geometries. 
Simultaneous Thermal Analysis System
Differential scanning calorimeter and thermal analysis DTA DSC TGA
  • NETZSCH STA449F3 system can perform thermogravimetric (TGA), differential scanning calorimetry (DSC) and differential thermal analysis (DTA) depending on the sample carrier installed. 
  • SiC furnace is capable of routine measurements to 1600 oC in a variety of inert, oxidizing, and corrosive atmospheres. 
  • Graphite furnace is capable of operation to 2000 oC in inert atmospheres. 
  • Triple mass flow controllers enable dynamic gas control during testing. 
Spark Plasma Sintering System
SUGA 630Sx spark plasma sintering setup showing the main chamber during high-heat operation, close-up of a glowing hot die, and various cylindrical and custom graphite dies.
  • SUGA 630Sx spark plasma sintering (SPS) or current assisted densification system. 
  • Maximum pressing load of 60 kN and 3000 A power supply capable of rapid   sintering under pyrometer control to 2200 oC. 
  • System is currently operated with 10 mm, 15 mm, 20 mm round dies, and a custom die set to produce lateral composition gradients. Other custom geometries are possible.   

Furnaces

Draco tube furnace
Antila Tube Furnace
Virgo Tube Furnace
Cassiopeia III Tube Furnace
Cassiopeia Tube Furnace
Columba Tube Furnace
Orionids Automated Thermal Cycling Furnace
Cassiopeia II Tube Furnace
Andromeda Box Furnace
Orion Box Furnace
Pegasus Box Furnace
Hydra Drying Oven
Scorpius
Pleiades Bottom Loading Box Furnace
  

Other Equipment

Roller Ball Mill
Polishing Wheel
Low Speed Diamond Wafering Saw
Planetary Ball Mill
Carver Press
Glove Box
Tube Sealing Setup
Olympus Microscope
Analytical Balances